BS ISO 13909-7:2016 – TC:2020 Edition
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Tracked Changes. Hard coal and coke. Mechanical sampling – Methods for determining the precision of sampling, sample preparation and testing
Published By | Publication Date | Number of Pages |
BSI | 2020 | 114 |
PDF Catalog
PDF Pages | PDF Title |
---|---|
66 | Foreword |
67 | Introduction |
69 | 1 Scope 2 Normative references 3 Terms and definitions 4 General |
70 | 5 Formulae relating to factors affecting precision 5.1 General |
71 | 5.2 Sampling |
72 | 6 Estimation of primary increment variance 6.1 Direct determination of individual primary increments |
73 | 6.2 Determination using the estimate of precision 7 Methods for estimating precision 7.1 General 7.2 Duplicate sampling with twice the number of increments |
76 | 7.3 Duplicate sampling during routine sampling |
77 | 7.4 Alternatives to duplicate sampling 7.5 Precision adjustment procedure |
78 | 8 Calculation of precision 8.1 Replicate sampling |
79 | 8.2 Normal sampling scheme |
80 | 9 Methods of checking sample preparation and testing errors 9.1 General 9.2 Target value for variance of sample preparation and analysis 9.2.1 General |
81 | 9.2.2 Off-line preparation 9.2.3 On-line preparation 9.3 Checking procedure as a whole |
82 | 9.4 Checking stages separately 9.4.1 General |
83 | 9.4.2 Procedure 1 |
86 | 9.4.3 Procedure 2 |
89 | 9.4.4 Interpretation of results |
90 | 9.5 Procedure for obtaining two samples at each stage 9.5.1 With a riffle 9.5.2 With a mechanical sample divider 9.6 Example |
94 | Annex A (informative) Variogram method for determining variance |
102 | Annex B (informative) Grubbs’ estimators method for determining sampling precision |
111 | Bibliography |