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BS ISO 13909-7:2016 – TC:2020 Edition

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Tracked Changes. Hard coal and coke. Mechanical sampling – Methods for determining the precision of sampling, sample preparation and testing

Published By Publication Date Number of Pages
BSI 2020 114
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PDF Catalog

PDF Pages PDF Title
66 Foreword
67 Introduction
69 1 Scope
2 Normative references
3 Terms and definitions
4 General
70 5 Formulae relating to factors affecting precision
5.1 General
71 5.2 Sampling
72 6 Estimation of primary increment variance
6.1 Direct determination of individual primary increments
73 6.2 Determination using the estimate of precision
7 Methods for estimating precision
7.1 General
7.2 Duplicate sampling with twice the number of increments
76 7.3 Duplicate sampling during routine sampling
77 7.4 Alternatives to duplicate sampling
7.5 Precision adjustment procedure
78 8 Calculation of precision
8.1 Replicate sampling
79 8.2 Normal sampling scheme
80 9 Methods of checking sample preparation and testing errors
9.1 General
9.2 Target value for variance of sample preparation and analysis
9.2.1 General
81 9.2.2 Off-line preparation
9.2.3 On-line preparation
9.3 Checking procedure as a whole
82 9.4 Checking stages separately
9.4.1 General
83 9.4.2 Procedure 1
86 9.4.3 Procedure 2
89 9.4.4 Interpretation of results
90 9.5 Procedure for obtaining two samples at each stage
9.5.1 With a riffle
9.5.2 With a mechanical sample divider
9.6 Example
94 Annex A (informative) Variogram method for determining variance
102 Annex B (informative) Grubbs’ estimators method for determining sampling precision
111 Bibliography
BS ISO 13909-7:2016 - TC
$258.95