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BSI PD CEN ISO/TR 11827:2016

$198.66

Textiles. Composition testing. Identification of fibres

Published By Publication Date Number of Pages
BSI 2016 68
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This Technical Report describes procedures for the identification of natural and man-made fibres, and may be used, when necessary, to coordinate with methods for the quantitative analysis of fibre blends.

PDF Catalog

PDF Pages PDF Title
9 Scope
Safety note
10 Normative references
Terms and definitions
Principle
11 Apparatus and preparation of solutions
Apparatus
Light Microscope, using transmitted light
Scanning Electron Microscope
Bunsen Burner or other flame source
Infrared Spectrometer
Attenuated Total Reflection (ATR) spectroscopy device
Fourier Transform Infrared (FT-IR) spectrometer
Melting Point device (heated block)
Differential Scanning Calorimeter (DSC)
Thermal Gravimetric Analysis (TGA) device (thermobalance)
Gravimetric device (density gradient column)
Energy Dispersive X-ray (EDX) device
Preparation of solutions
Sodium hydroxide and calcium oxide
Iodine/potassium iodine solution
Zinc chloride/iodine solution
Chlorine bleaching solution
Zinc chloride/formic acid solution
12 Sodium carbonate 0,25 % solution
Sodium hydroxide 5 % solution
Sulphuric acid 75 % solution
Chloroform/trichloroacetic acid solution
Ethanol / potassium hydroxide solution
Techniques
Microscopy
Light Microscopy
Scanning Electron Microscopy
Refractive Index
General
13 Mounting media
Factors governing refractive indices
Behaviour under polarised light
14 Flame tests
Burning Test
15 Chlorine detection test
Nitrogen detection test
Staining Tests
Colouration test with iodine/ potassium iodide solution
Xanthoproteic reaction
Solubility Tests
Polyester confirmation
16 Cellulose confirmation
Infrared Spectroscopy
General
Procedure
17 Pressed-disc Technique
Mulling
Solvent-cast Films
18 Melt-cast Films
Attenuated Total Reflection (ATR)
Diffuse Reflectance Spectroscopy
19 FT-IR Microscopy
Interpretation of Spectra
20 Thermal Analysis
Melting Point Determination
Differential Scanning Calorimetry (DSC)
General
21 Procedure
Temperature range
Heating rate
Control of atmosphere
Sample considerations
Reference materials
22 Identification
Thermal Gravimetric Methods (TGA)
Density measurement methods
Other Instrumental Methods
Energy Dispersive X-ray (EDX) analysis
23 Examples of procedures
Procedure using microscopy, solubility tests and FT-IR tests
Example n°1
24 Example n°2
25 Procedure using solubility tests (examples)
Example n°1
26 Example n°2
27 Procedure using combustion tests and melting point determina
Procedure using microscopy, FT-IR analysis and thermal analy
Case of polyethylene / polypropylene bicomponent fibre
Analysis by microscopy
28 FT-IR analysis
29 Thermal analysis (DSC)
Case of polyester / polyester bicomponent fibre (example)
Analysis by microscopy
30 FT-IR analysis
Thermal analysis (TGA and DSC)
BSI PD CEN ISO/TR 11827:2016
$198.66