BSI PD ISO/TS 21362:2018
$189.07
Nanotechnologies. Analysis of nano-objects using asymmetrical-flow and centrifugal field-flow fractionation
| Published By | Publication Date | Number of Pages |
| BSI | 2018 | 50 |
PDF Catalog
| PDF Pages | PDF Title |
|---|---|
| 2 | National foreword |
| 7 | Foreword |
| 8 | Introduction |
| 11 | 1 Scope 2 Normative references 3 Terms and definitions |
| 17 | 4 Symbols and abbreviated terms |
| 19 | 5 Principles of operation 5.1 Field-flow fractionation (General) |
| 20 | 5.2 Specific applications by applied field 5.2.1 Flow field |
| 21 | 5.2.2 Centrifugal field |
| 23 | 6 Method development for AF4 6.1 General |
| 24 | 6.2 Sample specifications |
| 25 | 6.3 Mobile phase specifications |
| 26 | 6.4 Fractionation 6.4.1 Channel and membrane selection |
| 28 | 6.4.2 Injection and relaxation 6.4.3 Optimizing flow conditions 6.4.4 Elution programme |
| 29 | 6.4.5 Using FFF theory to select initial flow settings |
| 30 | 7 Method development for CF3 7.1 General 7.2 Choice of mobile phase 7.3 Field strength selection 7.4 Field decay programme |
| 31 | 7.5 Channel flow rate selection 7.6 Calculation of the relaxation time 7.7 Calculation of sample injection delay 8 Analysis of nano-objects 8.1 General |
| 32 | 8.2 Online size analysis |
| 33 | 8.3 Online concentration analysis 8.3.1 General 8.3.2 Mass-based methods |
| 34 | 8.3.3 Number-based methods |
| 35 | 8.4 Online material identification or composition |
| 36 | 8.5 Off-line analysis (Fraction collection) 9 Qualification, performance criteria and measurement uncertainty 9.1 System qualification and quality control 9.1.1 Basic system qualification |
| 37 | 9.1.2 Focusing performance |
| 38 | 9.1.3 Flow rate of the carrier liquid 9.1.4 Separation field 9.2 Method performance criteria 9.2.1 Recovery |
| 39 | 9.2.2 Selectivity 9.2.3 Retention 9.2.4 Resolution 9.3 Method precision and measurement uncertainty |
| 40 | 10 General procedures for measurement of samples 10.1 General 10.2 Calibration of retention time for online size analysis 10.2.1 Calibration of the AF4 channel |
| 41 | 10.2.2 Calibration of AF4 retention time for online size measurements 10.3 AF4 general measurement procedure |
| 42 | 10.4 CF3 general measurement procedure |
| 43 | 11 Test report 11.1 General 11.2 Apparatus and measurement parameters 11.2.1 AF4 recording/reporting specifications |
| 44 | 11.2.2 CF3 recording/reporting specifications 11.3 Reporting test results |
| 45 | Bibliography |
