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ASTM-D5790 2006

$63.38

D5790-95(2006) Standard Test Method for Measurement of Purgeable Organic Compounds in Water by Capillary Column Gas Chromatography/Mass Spectrometry

Published By Publication Date Number of Pages
ASTM 2006 56
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1.1 This test method covers the identification and simultaneous measurement of purgeable volatile organic compounds. It has been validated for treated drinking water, wastewater, and ground water. This test method is not limited to these particular aqueous matrices; however, the applicability of this test method to other aqueous matrices must be demonstrated.

1.2 This test method is applicable to a wide range of organic compounds that have sufficiently high volatility and low water solubility to be efficiently removed from water samples using purge and trap procedures. lists the compounds that have been validated for this test method. This test method is not limited to the compounds listed in ; however, the applicability of the test method to other compounds must be demonstrated.

1.3 Analyte concentrations up to approximately 200 ?g/L may be determined without dilution of the sample. Analytes that are inefficiently purged from water will not be detected when present at low concentrations, but they can be measured with acceptable accuracy and precision when present in sufficient amounts.

1.4 Analytes that are not separated chromatographically, but that have different mass spectra and noninterfering quantitation ions, can be identified and measured in the same calibration mixture or water sample. Analytes that have very similar mass spectra cannot be individually identified and measured in the same calibration mixture or water sample unless they have different retention times. Coeluting compounds with very similar mass spectra, such as structural isomers, must be reported as an isomeric group or pair. Two of the three isomeric xylenes are examples of structural isomers that may not be resolved on the capillary column, and if not, must be reported as an isomeric pair.

1.5 It is the responsibility of the user to ensure the validity of this test method for untested matrices.

1.6 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Terminology
2 Summary of Test Method
Significance and Use
3 Interferences
TABLE 1
4 Apparatus
5 TABLE 2
6 Reagents and Materials
7 Hazards
Sample Collection, Preservation, and Storage
8 Calibration and Standardization
9 Procedure
11 Calculation
Quality Control
12 Precision and Bias
Keywords
TABLE 3
19 TABLE 4
26 TABLE 5
33 TABLE 6
40 TABLE 7
46 TABLE 8
53 X1. SUMMARY OF TCLP STATISTICS
54 TABLE X1.1
55 X2. INTERLABORATORY COLLABORATIVE STUDY INFORMATION
REFERENCES
TABLE X2.1
ASTM-D5790 2006
$63.38