BS EN 16620:2015
$102.76
Food analysis. Determination of furan in coffee and coffee products by headspace gas chromatography and mass spectrometry (HS GC-MS)
Published By | Publication Date | Number of Pages |
BSI | 2015 | 20 |
This European Standard specifies a method for the determination of furan in coffee and coffee products with headspace-gas chromatography-mass spectrometry (HS-GC-MS), see [1] and [2]. Coffee products in the scope of this method are extracts which have been spray-dried, agglomerated or freeze-dried. The method has been validated in an interlaboratory study via the analysis of naturally contaminated samples of spraydried coffee, freeze-dried coffee and ground roasted coffee ranging from 264 μg/kg to 2 840 μg/kg.
PDF Catalog
PDF Pages | PDF Title |
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5 | Foreword |
6 | 1 Scope 2 Normative references 3 Principle 4 Reagents |
7 | 5 Apparatus |
8 | 6 Procedure 6.1 Sample preparation 6.2 Estimation of furan content |
9 | 6.3 Standard addition analysis Table 1 — Example of a standard addition for an estimated furan content x0 of 2,5 µg/g 6.4 Determination with headspace-GC-MS |
11 | Table 2 — Ions for identification and quantification of furan (for more information see [3]) 7 Calculation 7.1 General |
12 | 8 Precision 8.1 General 8.2 Repeatability |
13 | 8.3 Reproducibility 9 Test report |
14 | Annex A (informative) Typical chromatograms |
15 | Figure A.1 — Typical chromatogram of furan and d4-furan |
16 | Annex B (informative) Precision data Table B.1 — Precision data for furan in coffee with headspace GC-MS |
17 | Bibliography |