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BS EN 16858:2017

$142.49

Foodstuffs. Determination of melamine and cyanuric acid in foodstuffs by liquid chromatography and tandem mass spectrometry (LC-MS/MS)

Published By Publication Date Number of Pages
BSI 2017 30
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This European Standard specifies a method for the determination of melamine and cyanuric acid in foodstuffs with liquid chromatography in combination with tandem mass spectrometry. The method has been validated in an interlaboratory study via the analysis of spiked samples of milk based infant formula, soy based infant formula, milk powder, whole milk, soy drink and milk chocolate ranging from 0,71 mg/kg to 1,43 mg/kg for melamine and 0,57 mg/kg to 1,45 mg/kg for cyanuric acid. The limits of quantification (LOQ) for melamine and cyanuric acid in food are 0,05 mg/kg and 0,25 mg/kg, respectively. The upper limit of the working range is up to 10 mg/kg for melamine and up to 25 mg/kg for cyanuric acid.

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 1 Scope
2 Normative references
3 Principle
4 Reagents
9 5 Apparatus
10 6 Procedure
11 7 System settings
16 8 Calculation and expression of results
19 9 Precision data
20 10 Test report
22 Annex A (informative)Typical HPLC chromatograms
26 Annex B (informative)Precision data
BS EN 16858:2017
$142.49