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BS EN ISO 12228-2:2014:2015 Edition

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Determination of individual and total sterols contents. Gas chromatographic method – Olive and olive pomace oils

Published By Publication Date Number of Pages
BSI 2015 26
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This part of ISO 12228 specifies a procedure for the gas chromatographic determination of the contents and composition of sterols and triterpene dialcohols in olive and olive pomace oils. For the determination of the contents and composition of sterols in all other animal and vegetable fats and oils, ISO 12228-1 is to be used.

NOTE This part of ISO 12228 is technically identical to IOC Standard COI/T.20/Doc. No. 30 (November 2011).

PDF Catalog

PDF Pages PDF Title
4 Foreword
6 Foreword
7 Section sec_1
Section sec_2
Section sec_3
Section sec_3.1
Section sec_3.2
Section sec_3.3
1 Scope
2 Normative references
3 Terms and definitions
8 Section sec_4
Section sec_5
Section sec_5.1
Section sec_5.2
Section sec_5.3
Section sec_5.4
Section sec_5.5
Section sec_5.6
Section sec_5.7
Section sec_5.8
Section sec_5.9
Section sec_5.10
Section sec_5.11
Section sec_5.12
4 Principle
5 Reagents
9 Section sec_5.13
Section sec_5.14
Section sec_5.15
Section sec_5.16
Section sec_5.17
Section sec_5.18
Section sec_5.19
Section sec_5.20
Section sec_6
Section sec_6.1
Section sec_6.2
Section sec_6.3
Section sec_6.4
Section sec_6.5
Section sec_6.6
Section sec_6.7
Section sec_6.8
Section sec_6.9
Section sec_6.10
6 Apparatus
10 Section sec_6.11
Section sec_6.12
Section sec_6.13
Section sec_6.14
Section sec_6.15
Section sec_6.16
Section sec_7
Section sec_7.1
Section sec_7.2
Section sec_8
Section sec_8.1
Section sec_8.2
Section sec_8.2.1
7 Sample
7.1 Sampling
7.2 Preparation of the test sample
8 Procedure
8.1 Test portion
8.2 Preparation of unsaponifiable matter
11 Section sec_8.2.2
Section sec_8.2.3
Section sec_8.2.4
Section sec_8.3
Section sec_8.3.1
Section sec_8.3.2
Section sec_8.3.3
Section sec_8.3.4
8.3 Separation of the sterol and triterpene dialcohols (erythrodiol, uvaol) fractions by TLC
12 Section sec_8.3.5
Section sec_8.3.6
Section sec_8.4
Section sec_8.4.1
Section sec_8.4.2
Section sec_8.5
Section sec_8.5.1
8.4 Preparation of the trimethylsilyl ethers
8.5 Gas chromatographic analysis
13 Section sec_8.5.2
Table tab_1
Section sec_9
Section sec_9.1
9 Expression of results
9.1 Quantitative evaluation
14 Section sec_9.2
Section sec_9.3
Section sec_9.4
9.2 Determination of the total sterol content
9.3 Composition of sterols
9.4 Composition of triterpene dialcohols
15 Section sec_10
Section sec_10.1
Section sec_10.2
Section sec_10.3
Section sec_11
10 Precision
10.1 Interlaboratory test
10.2 Repeatability limit, r 
10.3 Reproducibility limit, R 
11 Test report
16 Annex sec_A
Table tab_d
Figure fig_A.1
Annex A
(informative)

Figures

17 Figure fig_A.2
18 Figure fig_A.3
19 Annex sec_B
Table tab_B.1
Table tab_B.2
Annex B
(informative)

Interlaborative trial

20 Table tab_B.3
Table tab_B.4
Table tab_B.5
21 Table tab_B.6
Table tab_B.7
Table tab_B.8
22 Reference ref_1
Reference ref_2
Reference ref_3
Reference ref_4
Bibliography
BS EN ISO 12228-2:2014
$142.49