BS EN ISO 12228-2:2014:2015 Edition
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Determination of individual and total sterols contents. Gas chromatographic method – Olive and olive pomace oils
Published By | Publication Date | Number of Pages |
BSI | 2015 | 26 |
This part of ISO 12228 specifies a procedure for the gas chromatographic determination of the contents and composition of sterols and triterpene dialcohols in olive and olive pomace oils. For the determination of the contents and composition of sterols in all other animal and vegetable fats and oils, ISO 12228-1 is to be used.
NOTE This part of ISO 12228 is technically identical to IOC Standard COI/T.20/Doc. No. 30 (November 2011).
PDF Catalog
PDF Pages | PDF Title |
---|---|
4 | Foreword |
6 | Foreword |
7 | Section sec_1 Section sec_2 Section sec_3 Section sec_3.1 Section sec_3.2 Section sec_3.3 1 Scope 2 Normative references 3 Terms and definitions |
8 | Section sec_4 Section sec_5 Section sec_5.1 Section sec_5.2 Section sec_5.3 Section sec_5.4 Section sec_5.5 Section sec_5.6 Section sec_5.7 Section sec_5.8 Section sec_5.9 Section sec_5.10 Section sec_5.11 Section sec_5.12 4 Principle 5 Reagents |
9 | Section sec_5.13 Section sec_5.14 Section sec_5.15 Section sec_5.16 Section sec_5.17 Section sec_5.18 Section sec_5.19 Section sec_5.20 Section sec_6 Section sec_6.1 Section sec_6.2 Section sec_6.3 Section sec_6.4 Section sec_6.5 Section sec_6.6 Section sec_6.7 Section sec_6.8 Section sec_6.9 Section sec_6.10 6 Apparatus |
10 | Section sec_6.11 Section sec_6.12 Section sec_6.13 Section sec_6.14 Section sec_6.15 Section sec_6.16 Section sec_7 Section sec_7.1 Section sec_7.2 Section sec_8 Section sec_8.1 Section sec_8.2 Section sec_8.2.1 7 Sample 7.1 Sampling 7.2 Preparation of the test sample 8 Procedure 8.1 Test portion 8.2 Preparation of unsaponifiable matter |
11 | Section sec_8.2.2 Section sec_8.2.3 Section sec_8.2.4 Section sec_8.3 Section sec_8.3.1 Section sec_8.3.2 Section sec_8.3.3 Section sec_8.3.4 8.3 Separation of the sterol and triterpene dialcohols (erythrodiol, uvaol) fractions by TLC |
12 | Section sec_8.3.5 Section sec_8.3.6 Section sec_8.4 Section sec_8.4.1 Section sec_8.4.2 Section sec_8.5 Section sec_8.5.1 8.4 Preparation of the trimethylsilyl ethers 8.5 Gas chromatographic analysis |
13 | Section sec_8.5.2 Table tab_1 Section sec_9 Section sec_9.1 9 Expression of results 9.1 Quantitative evaluation |
14 | Section sec_9.2 Section sec_9.3 Section sec_9.4 9.2 Determination of the total sterol content 9.3 Composition of sterols 9.4 Composition of triterpene dialcohols |
15 | Section sec_10 Section sec_10.1 Section sec_10.2 Section sec_10.3 Section sec_11 10 Precision 10.1 Interlaboratory test 10.2 Repeatability limit, r 10.3 Reproducibility limit, R 11 Test report |
16 | Annex sec_A Table tab_d Figure fig_A.1 Annex A (informative) Figures |
17 | Figure fig_A.2 |
18 | Figure fig_A.3 |
19 | Annex sec_B Table tab_B.1 Table tab_B.2 Annex B (informative) Interlaborative trial |
20 | Table tab_B.3 Table tab_B.4 Table tab_B.5 |
21 | Table tab_B.6 Table tab_B.7 Table tab_B.8 |
22 | Reference ref_1 Reference ref_2 Reference ref_3 Reference ref_4 Bibliography |