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ASTM-E2253 2016

$40.63

E2253-16 Standard Test Method for Temperature and Enthalpy Measurement Validation of Differential Scanning Calorimeters

Published By Publication Date Number of Pages
ASTM 2016 8
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ASTM E2253-16

Historical Standard: Standard Test Method for Temperature and Enthalpy Measurement Validation of Differential Scanning Calorimeters

ASTM E2253

Scope

1.1 This test method provides procedures for validating temperature and enthalpy measurements of differential scanning calorimeters (DSC) and analytical methods based upon the measurement of temperature or enthalpy (or heat), or both, by DSC. Performance parameters determined include temperature and calorimetric repeatability (precision), detection limit, quantitation limit, linearity, and bias. This test method is applicable to exothermic events.

1.2 Validation of apparatus performance and analytical methods is requested or required for quality initiatives or where results may be used for legal purposes.

1.3 The values stated in SI units are to regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Keywords

detection limit; differential scanning calorimetry; enthalpy; linearity; precision; quantitation limit; range; repeatability; thermal analysis; validation;

ICS Code

ICS Number Code 17.200.10 (Heat. Calorimetry)

DOI: 10.1520/E2253-16

ASTM-E2253 2016
$40.63