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BS EN 12946:2023

$86.31

Liming materials. Determination of the calcium content and magnesium content. Complexometric method

Published By Publication Date Number of Pages
BSI 2023 14
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TThis document specifies a complexometric method for the determination of the calcium content and the magnesium content of liming materials. It is not applicable to products with a mass fraction less than 2 % magnesium or those with a mass fraction more than 1 % P2O5 and is not applicable to silicate liming materials.

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PDF Pages PDF Title
2 undefined
7 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
5.1 General
5.2 Hydrochloric acid solution
8 5.3 Hydrochloric acid solution
5.4 Hydrochloric acid solution
5.5 Standard calcium solution, containing 2,004 g of calcium per litre
5.6 Standard magnesium solution, containing 1,216 g of magnesium per litre
5.7 Ethylenediamine tetraacetic acid (EDTA) standard solution, c(EDTA) = 0,05 mol/l
5.8 Calcein thymolphthalein indicator
9 5.9 Calcon carbonic acid indicator
5.10 Eriochrome black T indicator
5.11 Triethanolamine
5.12 Buffer solution, pH 10,5
5.13 Sodium hydroxide solution
6 Apparatus
7 Sampling
8 Procedure
8.1 Preparation
8.1.1 Preparation of test sample
10 8.1.2 Preparation of test solution
8.2 Determination
8.2.1 Aliquot portion
8.2.2 Titration in the presence of eriochrome black T
8.2.3 Titration in the presence of calcein thymolphthalein or calcon carbonic acid
11 8.3 Control test of the standard solutions
9 Expression of results
10 Precision
10.1 General
12 10.2 Repeatability
10.3 Reproducibility
11 Test report
BS EN 12946:2023
$86.31