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BS EN 16651:2015

$102.76

Fertilizers. Determination of N-(n-Butyl)thiophosphoric acid triamide (NBPT) and N-(n-Propyl)thiophosphoric acid triamide (NPPT). Method using high-performance liquid chromatography (HPLC)

Published By Publication Date Number of Pages
BSI 2015 16
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This European Standard specifies a method for the quantitative determination of the urease inhibitors N-(n-Butyl)thiophosphoric acid triamide (NBPT, CAS-No. 94317-64-3) and N-(n-Propyl)thiophosphoric acid triamide (NPPT, CAS-No. 916809-14-8) content in urea based fertilizers using high-performance liquid chromatography (HPLC).

PDF Catalog

PDF Pages PDF Title
5 Foreword
6 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
7 6 Apparatus
8 Table 1 — Example of HPLC conditions a
7 Sampling
8 Procedure
8.1 Preparation of the test solution
8.2 Calibration
8.3 Blank test
8.4 Calculation and expression of the results0F )
8.4.1 Concentration of NBPT
9 8.4.2 Concentration of NPPT
8.4.3 External response factors
10 8.4.4 Calculation of the total content
8.5 Environmental aspects
9 Precision
9.1 Inter-laboratory test
9.2 Repeatability
9.3 Reproducibility
11 Table 2 — NPPT: Mean values, repeatability and reproducibility limits
Table 3 — NBPT: Mean values, repeatability and reproducibility limits
10 Test report
12 Annex A (informative) Results of the inter-laboratory test
Table A.1 — Statistical results of the inter-laboratory trial for NPPT
Table A.2 — Statistical results of the inter-laboratory trial for NBPT
13 Bibliography
BS EN 16651:2015
$102.76